CAS 101597-25-5 1,1-Bis(4-methoxyphenyl)-2-propyn-1-ol
NAME:1,1-Bis(4-methoxyphenyl)-2-propyn-1-ol CAS:101597-25-5 MF:C17H16O3 MW:268.31 PURITY:98% Worldwide Delivery Made in China
Categories:
Material Chemistry
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Product introduction
| NAME | 1,1-Bis(4-methoxyphenyl)-2-propyn-1-ol |
| CAS | 101597-25-5 |
| MF | C17H16O3 |
| MW | 268.31 |
| DENSITY | 1.156 |
| MP | 91.9-92.2℃ |
| EINECS | 1592732-453-0 |
| BP | 412.0±45.0 °C |
| STORAGE | 2-8°C |
Preparation Methods
Synthetic Routes and Reaction Conditions
The synthesis of 1,1-Bis(4-methoxyphenyl)prop-2-yn-1-ol typically involves the reaction of 4-methoxybenzaldehyde with propargyl alcohol in the presence of a base such as sodium hydroxide. The reaction proceeds through a nucleophilic addition mechanism, resulting in the formation of the desired product. The reaction conditions often include refluxing the mixture in a suitable solvent like ethanol or methanol for several hours to ensure complete conversion.
Industrial Production Methods
On an industrial scale, the production of this compound may involve similar synthetic routes but with optimized reaction conditions to enhance yield and purity. The use of continuous flow reactors and advanced purification techniques such as recrystallization and chromatography can be employed to achieve high-quality products.
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