CAS 195447-25-7 1-BOC-3,3-DIFLUOROPYRROLIDINE
NAME:1-BOC-3,3-DIFLUOROPYRROLIDINE CAS:195447-25-7 MF:C9H15F2NO2 MW:207.22 PURITY:98% Worldwide Delivery Made in China
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Material Chemistry
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Product introduction
| NAME | 1-BOC-3,3-DIFLUOROPYRROLIDINE |
| CAS | 195447-25-7 |
| MF | C9H15F2NO2 |
| MW | 207.22 |
| STORAGE | 2-8°C |
Preparation Methods
Synthetic Routes and Reaction Conditions
The synthesis of tert-Butyl 3,3-difluoropyrrolidine-1-carboxylate typically involves the reaction of 3,3-difluoropyrrolidine with tert-butyl chloroformate. The reaction is carried out in the presence of a base such as triethylamine in an organic solvent like dichloromethane. The reaction mixture is stirred at room temperature for several hours, followed by purification through column chromatography to obtain the desired product .
Industrial Production Methods
Industrial production of tert-Butyl 3,3-difluoropyrrolidine-1-carboxylate follows similar synthetic routes but on a larger scale. The process involves the use of automated reactors and continuous flow systems to ensure consistent product quality and yield. The reaction conditions are optimized to minimize by-products and maximize the efficiency of the synthesis .
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